Browsing by Author "Masuda, Jason Douglas, 1977-"

Browsing by Author "Masuda, Jason Douglas, 1977-"

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    1,3-Bis(2,6-diisopropylphenyl)-2-trichloromethylimidazolidine 
    Stack, Darcie L.; Masuda, Jason Douglas, 1977- (MDPI, 2017-10-12)
    A new chloroform adduct of the N-heterocyclic carbene (NHC) 1,3-bis(2,6-diisopropylphenyl)imidazolidin-2-ylidene (SIPr) has been prepared via C–H bond activation of the chloroform at the carbene carbon. This redox ...

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    1,3-Bis(2,6-diisopropylphenyl)-imidazolidin-2-ylidene 
    Masuda, Jason Douglas, 1977-; Giffin, Nick A.; Hendsbee, Arthur D. (International Union of Crystallography, 2010-09)
    The title compound, C[subscript 27]H[subscript 38]N[subscript 2], is the first reported free imidazolidin-2-ylidene carbene with 2,6-diisopropylphenyl groups in the 1,3-positions. The five-membered ring adopts a twisted ...

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    1-(2,4,6-Triisopropylphenyl)ethanone 
    Masuda, Jason Douglas, 1977-; Blair, Amber D.; Hendsbee, Arthur D. (International Union of Crystallography, 2011-10)
    The title compound, C[subscript 17]H[subscript 26]O, is a di-ortho-alkyl substituted phenyl ethanone that exhibits a significant twisting of the ketone fragment relative to the aromatic ring [O—C—C—C torsion angle = 89.32 ...

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    1-(2,4,6-Triisopropylphenyl)ethanone 
    Blair, Amber D.; Hendsbee, Arthur D.; Masuda, Jason Douglas, 1977- (Wiley-Blackwell, 2011-10)
    The title compound, C17H26O, is a di-ortho-alkyl substituted phenyl ethanone that exhibits a significant twisting of the ketone fragment relative to the aromatic ring [O—C—C—C torsion ...

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    3-Methylthiobenzamide 
    Khan, Mahmood-ul-Hassan; Hameed, Shahid; Akhtar, Tashfeen; Masuda, Jason Douglas, 1977- (International Union of Crystallography, 2009-06)
    In the title compound, C[subscript 8]H[subscript 9]NS, the dihedral angle between the aromatic ring and the thioamide fragment is 36.0 (2)[degrees ]. There are [pi]-stacking interactions between coplanar aryl fragments, ...

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    4-Bromothiobenzamide 
    Khan, Mahmood-ul-Hassan; Hameed, Shahid; Akhtar, Tashfeen; Masuda, Jason Douglas, 1977- (International Union of Crystallography, 2009)
    The title compound, C[subscript 7]H[subscript 6]BrNS, crystallizes with two molecules in the asymmetric unit. The dihedral angles between the aromatic ring and the thioamide fragment are 23.6 (4) and 20.5 (3)[degrees] in ...

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    4-Chlorobenzothioamide 
    Khan, Mahmood-ul-Hassan; Hameed, Shahid; Akhtar, Tashfeen; Masuda, Jason Douglas, 1977- (International Union of Crystallography, 2009)
    In the title compound, C[subscript 7]H[subscript 6]ClNS, the dihedral angle between the aromatic ring and the thioamide fragment is 28.1 (2)[degrees]. The structure features a [pi]-stacking interaction between the aromatic ...

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    Anhydrous TEMPO-H: reactions of a good hydrogen atom donor with low-valent carbon centres 
    Giffin, Nick A.; Makramalla, Miller; Hendsbee, Arthur D.; Robertson, Katherine N.; Sherren, Cody; Pye, Cory C.; Masuda, Jason Douglas, 1977-; Clyburne, Jason A. C. (Royal Society of Chemistry, 2011)
    In this paper, we report a novel synthesis of anhydrous 1-hydroxy-2,2,6,6-tetramethyl-piperidine (TEMPO-H). An X-ray crystal structure and full characterization of the compound are included. Compared to hydrated TEMPO-H, ...

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    Biphenyl substituted cyclopentadienyl ligand complexes 
    Ramgoolam, Ketnavi (Halifax, N.S. : Saint Mary's University, 2019)
    The synthesis of biphenyl substituted cyclopentadienyl ligands are described. The synthetic route is accomplished through the reaction of aryl lithium reagents with cobaltocenium salts, followed by oxidation of the ...

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    Controlling the Thermal Stability and Volatility of Organogold(I) Compounds for Vapor Deposition with Complementary Ligand Design 
    Griffiths, Matthew B. E.; Dubrawski, Zachary S.; Bačić, Goran; Japahuge, Achini; Masuda, Jason Douglas, 1977-; Zeng, Tao; Barry, Seán T. (Wiley, 2019-12-15)
    Atomic layer deposition (ALD) of gold is being studied by multiple research groups, but to date no process using non-energetic co-reactants has been demonstrated. In order to access milder co-reactants, precursors with ...

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    Crystal structure determination as part of an ongoing undergraduate organic laboratory project: 5-[(E)-styryl]-1,3,4-oxathiazol-2-one 
    Nason, Trevor R.; Schriver, Melbourne J.; Hendsbee, Arthur D.; Masuda, Jason Douglas, 1977- (International Union of Crystallography, 2017-08-04)
    The title compound, C10H7NO2S, provides the first structure of an α-alkenyl oxathiazolone ring. The phenyl ring and the oxa­thia­zolone groups make dihedral angles of 0.3 (3) ...

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    Crystal structure of 2-azido-1,3-bis(2,6-diiso- propylphenyl)-1,3,2-diazaphospholidine 
    Veinot, Alex J.; Blair, Amber D.; Masuda, Jason Douglas, 1977- (International Union of Crystallography, 2017-05-31)
    The title compound, C26H38N5P, was synthesized by reacting 2-chloro-1,3- bis(2,6-diisopropylphenyl)-1,3,2-diazaphospholidine with sodium azide and a catalytic amount of lithium chloride in ...

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    Crystal structure of 2-chloro-1,3-(2,6-diisopropylphenyl)- 4,5-dihydro-1H-imidazol-3-ium tetrakis- (3,5-trifluoromethylphenyl)borate 
    Stack, Darcie L.; Masuda, Jason Douglas, 1977- (International Union of Crystallography, 2016-10)
    The title compound, C [subscript 27] H[subscript 38]ClN[subscript 2] [superscript +][centre dot]C[subscript 32]H[subscript 12]BF[subscript 24][superscript -], was synthesized by reacting the product formed from a previous ...

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    Crystal structure of 2-chloro-1,3-bis(2,6-diiso- propylphenyl)-1,3,2-diazaphospholidine 2-oxide 
    Veinot, Alex J.; Hendsbee, Arthur D.; Masuda, Jason Douglas, 1977- (International Union of Crystallography, 2017-04-21)
    The title compound, C26H38ClN2OP, was synthesized by reacting phosphoryl chloride with N,N′-bis­(2,6-diiso­propyl­phen­yl)ethane-1 ...

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    Crystal Structure of Bis(2,4,6-trimethylphenyl)-phosphine Oxide 
    Veinot, Alex J.; Ramgoolam, Ketnavi; Giffin, Nick A.; Masuda, Jason Douglas, 1977- (MDPI, 2017-09-19)
    The single crystal structure of bis(2,4,6-trimethylphenyl) phosphine oxide has been determined. All interatomic distances and angles can be considered normal. The aryl substituents adopt an intermediate configuration when ...

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    The crystal structures of two isomers of 5-(phenyl- isothiazolyl)-1,3,4-oxathiazol-2-one 
    Zhu, Shuguang; Schriver, Melbourne J.; Hendsbee, Arthur D.; Masuda, Jason Douglas, 1977- (International Union of Crystallography, 2017-11-01)
    The syntheses and crystal structures of two isomers of phenyl iso­thia­zolyl oxa­thia­zolone, C11H6N2O2S2, are described [systematic names: ...

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    Cyclic alkyl phosphino carbenes – a synthetic investigation 
    Wortman, Benjamin (Halifax, N.S. : Saint Mary's University, 2023-04-19)
    A proposed synthetic pathway to produce a cyclic (alkyl)(phosphino) carbene (CAPC)has been investigated. 1-bromo-2,4,6-tritertbutylbenzene (-2,4,6-tritertbutylbenzene =mes*) was used to produce Mes*PCl2. A ring ...

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    ([eta superscript 5]-Cyclopentadienyl)([eta superscript 6]-1,2-dipyrrolidin-1-ylbenzene)iron(II) hexafluoridophosphate 
    Jenkins, Hilary A.; Masuda, Jason Douglas, 1977-; Piorko, Adam (International Union of Crystallography, 2009)
    Both complexed rings in the iron(II) complex cation of the title salt, [Fe(C[subscript 5]H[subscript 5])(C[subscript 14]H[subscript 20]N[subscript 2])]PF[subscript 6], are almost parallel [dihedral angle between planes = ...

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    ([eta superscript 5]-Cyclopentadienyl)([eta superscript 6]-phenoxathiin 10,10-dioxide)iron(II) hexafluoridophosphate and phenoxathiin 10,10-dioxide 
    Hendsbee, Arthur D.; Masuda, Jason Douglas, 1977-; Piorko, Adam (International Union of Crystallography, 2011-11)
    In the structure of the title complex salt, [Fe(C[subscript 5]H[subscript 5])(C[subscript 12]H[subscript 8]O[subscript 3]S)]PF[subscript 6], the coordinated cyclopentadienyl (Cp) and benzene ring planes are almost parallel, ...

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    ([eta superscript 5]-Cyclopentadienyl)[(1,2,3,4,4a,10a-[eta])-1-methylthianthrene]iron(II) hexafluoridophosphate acetone 0.33-solvate 
    Hendsbee, Arthur D.; Masuda, Jason Douglas, 1977-; Piorko, Adam (2009-11)
    The title complex salt, [Fe(C[subscript 5]H[subscript 5])(C[subscript 13]H[subscript 10]S[subscript 2])]PF[subscript 6][middle dot]0.33C[subscript 3]H[subscript 6]O, obtained from an acetone–diethyl ether–dichloromethane ...