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Browsing by Author "Hendsbee, Arthur D."

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1,3-Bis(2,6-diisopropylphenyl)-imidazolidin-2-ylidene

Masuda, Jason Douglas, 1977-; Giffin, Nick A.; Hendsbee, Arthur D. (International Union of Crystallography, 2010-09)

The title compound, C[subscript 27]H[subscript 38]N[subscript 2], is the first reported free imidazolidin-2-ylidene carbene with 2,6-diisopropylphenyl groups in the 1,3-positions. The five-membered ring adopts a twisted ...
1-(2,4,6-Triisopropylphenyl)ethanone

Masuda, Jason Douglas, 1977-; Blair, Amber D.; Hendsbee, Arthur D. (International Union of Crystallography, 2011-10)

The title compound, C[subscript 17]H[subscript 26]O, is a di-ortho-alkyl substituted phenyl ethanone that exhibits a significant twisting of the ketone fragment relative to the aromatic ring [O—C—C—C torsion angle = 89.32 ...
1-(2,4,6-Triisopropylphenyl)ethanone

Blair, Amber D.; Hendsbee, Arthur D.; Masuda, Jason Douglas, 1977- (Wiley-Blackwell, 2011-10)

The title compound, C₁₇H₂₆O, is a di-ortho-alkyl substituted phenyl ethanone that exhibits a significant twisting of the ketone fragment relative to the aromatic ring [O—C—C—C torsion ...
Anhydrous TEMPO-H: reactions of a good hydrogen atom donor with low-valent carbon centres

Giffin, Nick A.; Makramalla, Miller; Hendsbee, Arthur D.; Robertson, Katherine N.; Sherren, Cody; Pye, Cory C.; Masuda, Jason Douglas, 1977-; Clyburne, Jason A. C. (Royal Society of Chemistry, 2011)

In this paper, we report a novel synthesis of anhydrous 1-hydroxy-2,2,6,6-tetramethyl-piperidine (TEMPO-H). An X-ray crystal structure and full characterization of the compound are included. Compared to hydrated TEMPO-H, ...
Crystal structure determination as part of an ongoing undergraduate organic laboratory project: 5-[(E)-styryl]-1,3,4-oxathiazol-2-one

Nason, Trevor R.; Schriver, Melbourne J.; Hendsbee, Arthur D.; Masuda, Jason Douglas, 1977- (International Union of Crystallography, 2017-08-04)

The title compound, C¹⁰H⁷NO²S, provides the first structure of an α-alkenyl oxathiazolone ring. The phenyl ring and the oxathiazolone groups make dihedral angles of 0.3 (3) ...
Crystal structure of 2-chloro-1,3-bis(2,6-diiso- propylphenyl)-1,3,2-diazaphospholidine 2-oxide

Veinot, Alex J.; Hendsbee, Arthur D.; Masuda, Jason Douglas, 1977- (International Union of Crystallography, 2017-04-21)

The title compound, C₂₆H₃₈ClN₂OP, was synthesized by reacting phosphoryl chloride with N,N^′-bis(2,6-diisopropylphenyl)ethane-1 ...
The crystal structures of two isomers of 5-(phenyl- isothiazolyl)-1,3,4-oxathiazol-2-one

Zhu, Shuguang; Schriver, Melbourne J.; Hendsbee, Arthur D.; Masuda, Jason Douglas, 1977- (International Union of Crystallography, 2017-11-01)

The syntheses and crystal structures of two isomers of phenyl isothiazolyl oxathiazolone, C₁₁H₆N₂O₂S₂, are described [systematic names: ...
([eta superscript 5]-Cyclopentadienyl)([eta superscript 6]-phenoxathiin 10,10-dioxide)iron(II) hexafluoridophosphate and phenoxathiin 10,10-dioxide

Hendsbee, Arthur D.; Masuda, Jason Douglas, 1977-; Piorko, Adam (International Union of Crystallography, 2011-11)

In the structure of the title complex salt, [Fe(C[subscript 5]H[subscript 5])(C[subscript 12]H[subscript 8]O[subscript 3]S)]PF[subscript 6], the coordinated cyclopentadienyl (Cp) and benzene ring planes are almost parallel, ...
([eta superscript 5]-Cyclopentadienyl)[(1,2,3,4,4a,10a-[eta])-1-methylthianthrene]iron(II) hexafluoridophosphate acetone 0.33-solvate

Hendsbee, Arthur D.; Masuda, Jason Douglas, 1977-; Piorko, Adam (2009-11)

The title complex salt, [Fe(C[subscript 5]H[subscript 5])(C[subscript 13]H[subscript 10]S[subscript 2])]PF[subscript 6][middle dot]0.33C[subscript 3]H[subscript 6]O, obtained from an acetone–diethyl ether–dichloromethane ...
([eta superscript 5]-Cyclopentadienyl)[(1,2,3,4,4a,12a-[eta])-naphtho[2,3-b][1,4]benzodioxine]iron(II) hexafluoridophosphate

Hendsbee, Arthur D.; Masuda, Jason Douglas, 1977-; Piorko, Adam (International Union of Crystallography, 2010-09)

At 296 (2) K, both complexed rings in the iron(II) complex cation of the title salt, [Fe(C[subscript 5]H[subscript 5])(C[subscript 16]H[subscript 10]O[subscript 2])]PF[subscript 6], are almost parallel [dihedral angle ...
([eta superscript 5]-Cyclopentadienyl)[(1,2,3,4,4a,12a-[eta])-naphtho[2,3-b][1,4]benzodioxine]iron(II) hexafluoridophosphate

Masuda, Jason Douglas, 1977-; Piorko, Adam; Hendsbee, Arthur D. (International Union of Crystallography, 2010-09)

At 296 (2) K, both complexed rings in the iron(II) complex cation of the title salt, [Fe(C[subscript 5]H[subscript 5])(C[subscript 16]H[subscript 10]O[subscript 2])]PF[subscript 6], are almost parallel [dihedral angle ...
[[eta superscript 6]-1-Chloro-2-(pyrrolidin-1-yl)-benzene]([eta superscript 5]-cyclopentadienyl)iron(II) hexafluoridophosphate and ([eta superscript 5]-cyclopentadienyl){2-[[eta superscript 6]-2-(pyrrolidin-1-yl)-phenyl]phenol}iron(II) hexafluoridophosphate

Hendsbee, Arthur D.; Masuda, Jason Douglas, 1977-; Piorko, Adam (International Union of Crystallography, 2011-12)

In the complex salt [eta superscript 6]-1-chloro-2-(pyrrolidin-1-yl)benzene]-([eta superscript 5]-cyclopentadienyl)iron(II) hexafluoridophosphate, [Fe(C[subscript 5]H[subscript 5])-(C[subscript 10]H[subscript 12]CIN)]PF[subscript ...
A new polymorph of 2,6-bis(trifluoromethyl)benzoic acid

Masuda, Jason Douglas, 1977-; Giffin, Nick A.; Hendsbee, Arthur D. (International Union of Crystallography, 2011-05)

The asymmetric unit of a second polymorph of the title compound, C[subscript 9]H[subscript 4]F[subscript 6]O[subscript 2], contains five independent molecules, which form hydrogen-bonded O—H[ellipsis]O dimers about inversion ...
Reaction of sterically encumbered phenols, TEMPO-H, and organocarbonyl insertion reactions with L-AlH[subscript2] (L = HC(MeCNDipp)[subscript2], Dipp = 2,6- diisopropylphenyl)

Keyes, Lauren K.; Todd, Angela D. K.; Giffin, Nick A.; Veinot, Alex J.; Hendsbee, Arthur D.; Robertson, Katherine N.; Geier, Stephen J.; Masuda, Jason Douglas, 1977- (Royal Society of Chemistry, 2017-07-26)

2 (L = HC(MeCNDipp)₂, Dipp = 2,6-diisopropylphenyl) with sterically bulky phenols (2,4,6-trimethylphenol, MesOH; 2,6-diisopropylphenol, DippOH) and an N-hydroxylamine ...

Browsing by Author "Hendsbee, Arthur D."

Browsing by Author "Hendsbee, Arthur D."

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