Browsing Articles by Subject "Heterocyclic compounds"

Now showing items 1-11 of 11

1,3-Bis(2,6-diisopropylphenyl)-2-trichloromethylimidazolidine

Stack, Darcie L.; Masuda, Jason Douglas, 1977- (MDPI, 2017-10-12)

A new chloroform adduct of the N-heterocyclic carbene (NHC) 1,3-bis(2,6-diisopropylphenyl)imidazolidin-2-ylidene (SIPr) has been prepared via C–H bond activation of the chloroform at the carbene carbon. This redox ...
[(5a,6,7,8,9,9a-[eta superscript 6])-[l,4]Benzodioxinol[2,3-b]- pyridine]([eta superscript 5]cyclopentadienyl)iron(II) hexafluorophosphate

Piorko, Adam; Christie, Sean; Zaworotko, Michael J. (International Union of Crystallography, 1994-10)

The structure of [(5a,6,7,8,9,9a-[eta superscript 6])-[1,4]benzodi-oxino[2,3-b]pyridine]([eta superscript 5]-cyclopentadienyl)iron(II)hexafluorophosphate, [Fe(C[subscript 5]H[subscript 5])(C[subscript 11] H[subscript ...
Anhydrous TEMPO-H: reactions of a good hydrogen atom donor with low-valent carbon centres

Giffin, Nick A.; Makramalla, Miller; Hendsbee, Arthur D.; Robertson, Katherine N.; Sherren, Cody; Pye, Cory C.; Masuda, Jason Douglas, 1977-; Clyburne, Jason A. C. (Royal Society of Chemistry, 2011)

In this paper, we report a novel synthesis of anhydrous 1-hydroxy-2,2,6,6-tetramethyl-piperidine (TEMPO-H). An X-ray crystal structure and full characterization of the compound are included. Compared to hydrated TEMPO-H, ...
Crystal structure of 2-chloro-1,3-(2,6-diisopropylphenyl)- 4,5-dihydro-1H-imidazol-3-ium tetrakis- (3,5-trifluoromethylphenyl)borate

Stack, Darcie L.; Masuda, Jason Douglas, 1977- (International Union of Crystallography, 2016-10)

The title compound, C [subscript 27] H[subscript 38]ClN[subscript 2] [superscript +][centre dot]C[subscript 32]H[subscript 12]BF[subscript 24][superscript -], was synthesized by reacting the product formed from a previous ...
Crystal structure of 2-chloro-1,3-bis(2,6-diiso- propylphenyl)-1,3,2-diazaphospholidine 2-oxide

Veinot, Alex J.; Hendsbee, Arthur D.; Masuda, Jason Douglas, 1977- (International Union of Crystallography, 2017-04-21)

The title compound, C₂₆H₃₈ClN₂OP, was synthesized by reacting phosphoryl chloride with N,N^′-bis(2,6-diisopropylphenyl)ethane-1 ...
([eta superscript 5]-Cyclopentadienyl)([eta superscript 6]-phenoxathiin 10,10-dioxide)iron(II) hexafluoridophosphate and phenoxathiin 10,10-dioxide

Hendsbee, Arthur D.; Masuda, Jason Douglas, 1977-; Piorko, Adam (International Union of Crystallography, 2011-11)

In the structure of the title complex salt, [Fe(C[subscript 5]H[subscript 5])(C[subscript 12]H[subscript 8]O[subscript 3]S)]PF[subscript 6], the coordinated cyclopentadienyl (Cp) and benzene ring planes are almost parallel, ...
([eta superscript 5]-Cyclopentadienyl)[(1,2,3,4,4a,10a-[eta superscript 6])- 2-methylthianthrene]iron(II) hexafluorophosphate

Christie, Sean; Piorko, Adam; Zaworotko, Michael J. (International Union of Crystallography, 1994-12)

The structure of the title compound, [Fe(C[subscript 5]H[subscript 5])(C[subscript 13]H[subscript 10]-S[subscript 2])].PF[subscript 6], (I), has been studied. The dihedral angle between the outer benzene rings of the ligand ...
([eta superscript 5]-Cyclopentadienyl)[(1,2,3,4,4a,10a-[eta])-1-methylthianthrene]iron(II) hexafluoridophosphate acetone 0.33-solvate

Hendsbee, Arthur D.; Masuda, Jason Douglas, 1977-; Piorko, Adam (2009-11)

The title complex salt, [Fe(C[subscript 5]H[subscript 5])(C[subscript 13]H[subscript 10]S[subscript 2])]PF[subscript 6][middle dot]0.33C[subscript 3]H[subscript 6]O, obtained from an acetone–diethyl ether–dichloromethane ...
Structure of ([eta superscript 5]-cyclopentadienyl)(1,2,3,4,4a,10a-[eta superscript 6]-2-methyldibenzo[b,e][1,4)dioxine)iron(II) hexafluorophosphate at 163K

Abboud, K. A.; Simonsen, S. H.; Piorko, Adam; Sutherland, R. G. (International Union of Crystallography, 1991-06)

[C[subscript 18]H[subscript 15]Fe0[subscript 2]][PF[subscript 6]] (1), Mr = 464.13, monoclinic, P2[subscript 1]/c, a=7.976 (1), b =8.959 (3), c =24.936 (8) [Angstrom], [Beta] = 99.00 (2) °, V = 1760 (1) [Angstrom superscript ...
Structure of ([eta superscript 5]-cyclopentadienyl)([eta superscript 6]-thianthrene)iron(ll) hexafluorophosphate

Abboud, K. A.; Lynch, V. M.; Simonsen, S. H.; Piorko, Adam; Sutherland, R. G. (International Union of Crystallography, 1990-06)

[Fe(C₅H₅)(C₁₂H₈S₂)][PF₆] (I), M_r = 482.22, monoclinic, P2₁/c, a= 14.194 (3), b = 9.617 (2), c = 25-971 (5) Å,β = 100.31 (2)°, ...
Structure of the hexafluorophosphate salts of [mu]-([eta superscript 6]:[eta superscript 6]-phenoxazine)bis[[eta superscript 5]-cyclopentadienyliron(lI)] (1) and ([eta superscript 5]-cyclopentadienyl)([eta superscript 6]-phenoxathiin)iron(II) (2)

Lynch, V. M.; Thomas, S. N.; Simonsen, S. H.; Piorko, Adam; Sutherland, R. G. (International Union of Crystallography, 1986-09)

(1): [C[subscript 22]H[subscript 19]Fe[subscript 2]NO](PF[subscript 6])[subscript 2], M[subscript r] = 715.05, monoclinic, P2[subscript 1]/n, a = 10.635 (2), b = 9.928 (1), c = 22.562(7) [Angstrom], [beta] = 92.41 (1) °, ...